1,2,6-Thiadiazine 1-Oxides : Unsaturated Three-Dimensional S,N-Heterocycles from Sulfonimidamides
| dc.contributor.author | Schöbel, Jan-Hendrik | |
| dc.contributor.author | Passia, Marco Thomas | |
| dc.contributor.author | Wolter, Nadja Anna | |
| dc.contributor.author | Puttreddy, Rakesh | |
| dc.contributor.author | Rissanen, Kari | |
| dc.contributor.author | Bolm, Carsten | |
| dc.date.accessioned | 2020-05-04T12:35:21Z | |
| dc.date.available | 2020-05-04T12:35:21Z | |
| dc.date.issued | 2020 | |
| dc.identifier.citation | Schöbel, J.-H., Passia, M. T., Wolter, N. A., Puttreddy, R., Rissanen, K., & Bolm, C. (2020). 1,2,6-Thiadiazine 1-Oxides : Unsaturated Three-Dimensional S,N-Heterocycles from Sulfonimidamides. <i>Organic Letters</i>, <i>12</i>(7), 2702-2706. <a href="https://doi.org/10.1021/acs.orglett.0c00666" target="_blank">https://doi.org/10.1021/acs.orglett.0c00666</a> | |
| dc.identifier.other | CONVID_34973279 | |
| dc.identifier.uri | https://jyx.jyu.fi/handle/123456789/68819 | |
| dc.description.abstract | Unprecedented three-dimensional 1,2,6-thiadiazine 1-oxides have been prepared by an aza-Michael-addition/cyclization/condensation reaction sequence starting from sulfonimidamides and propargyl ketones. The products have been further functionalized by standard cross-coupling reactions, selective bromination of the heterocyclic ring, and conversion into a β-hydroxy substituted derivative. A representative product was characterized by single-crystal X-ray structure analysis. | en |
| dc.format.mimetype | application/pdf | |
| dc.language | eng | |
| dc.language.iso | eng | |
| dc.publisher | American Chemical Society | |
| dc.relation.ispartofseries | Organic Letters | |
| dc.rights | In Copyright | |
| dc.subject.other | sulfonimidamides | |
| dc.subject.other | single-crystal X-ray | |
| dc.title | 1,2,6-Thiadiazine 1-Oxides : Unsaturated Three-Dimensional S,N-Heterocycles from Sulfonimidamides | |
| dc.type | article | |
| dc.identifier.urn | URN:NBN:fi:jyu-202005043038 | |
| dc.contributor.laitos | Kemian laitos | fi |
| dc.contributor.laitos | Department of Chemistry | en |
| dc.contributor.oppiaine | Orgaaninen kemia | fi |
| dc.contributor.oppiaine | Soveltavan kemian yksikkö | fi |
| dc.contributor.oppiaine | Organic Chemistry | en |
| dc.contributor.oppiaine | The Unit of Applied Chemistry | en |
| dc.type.uri | http://purl.org/eprint/type/JournalArticle | |
| dc.type.coar | http://purl.org/coar/resource_type/c_2df8fbb1 | |
| dc.description.reviewstatus | peerReviewed | |
| dc.format.pagerange | 2702-2706 | |
| dc.relation.issn | 1523-7060 | |
| dc.relation.numberinseries | 7 | |
| dc.relation.volume | 12 | |
| dc.type.version | acceptedVersion | |
| dc.rights.copyright | © 2020 American Chemical Society | |
| dc.rights.accesslevel | openAccess | fi |
| dc.relation.grantnumber | 298817 | |
| dc.subject.yso | bioaktiiviset yhdisteet | |
| dc.format.content | fulltext | |
| jyx.subject.uri | http://www.yso.fi/onto/yso/p28433 | |
| dc.rights.url | http://rightsstatements.org/page/InC/1.0/?language=en | |
| dc.relation.doi | 10.1021/acs.orglett.0c00666 | |
| dc.relation.funder | Research Council of Finland | en |
| dc.relation.funder | Suomen Akatemia | fi |
| jyx.fundingprogram | Postdoctoral Researcher, AoF | en |
| jyx.fundingprogram | Tutkijatohtori, SA | fi |
| jyx.fundinginformation | We thank the Alexander von Humboldt Foundation for support of K.R. (AvH research award), and we gratefully acknowledge Marcus Frings (RWTH Aachen University) for measuring the HPLC data. Further thanks go to Daniela Lutsch (RWTH Aachen University) for supporting practical experiments. Financial support from the Academy of Finland (RP Grant No. 298817) is also gratefully acknowledged. | |
| dc.type.okm | A1 |
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