N-[2-(2,2-Dimethylpropanamido)- pyrimidin-4-yl]-2,2-dimethyl- propanamide n-hexane 0.25-solvate hemihydrate
| dc.contributor.author | Osmialowski, Borys | |
| dc.contributor.author | Valkonen, Arto | |
| dc.contributor.author | Checinska, Lilianna | |
| dc.date.accessioned | 2013-10-15T05:44:21Z | |
| dc.date.available | 2013-10-15T05:44:21Z | |
| dc.date.issued | 2013 | |
| dc.identifier.citation | Osmialowski, B., Valkonen, A., & Checinska, L. (2013). N-[2-(2,2-Dimethylpropanamido)- pyrimidin-4-yl]-2,2-dimethyl- propanamide n-hexane 0.25-solvate hemihydrate. <i>Acta Crystallographica Section E : Structure Reports Online</i>, <i>69</i>(11), o1617-o1618. <a href="https://doi.org/10.1107/S160053681302713X" target="_blank">https://doi.org/10.1107/S160053681302713X</a> | |
| dc.identifier.other | CONVID_22815784 | |
| dc.identifier.other | TUTKAID_57777 | |
| dc.identifier.uri | https://jyx.jyu.fi/handle/123456789/42333 | |
| dc.description.abstract | The asymmetric unit of the title compound, C₁₄H₂₂N₄O₂·0.25C₆H₁₄·0.5H₂O, contains two independent molecules of 2,4-bis(pivaloylamino)pyrimidine (M) with similar conformations, one water molecule and one-half n-hexane solvent molecule situated on an inversion center. In one independent M molecule, one of the two tert-butyl groups is rotationally disordered between two orientations in a 3:2 ratio. The n-hexane solvent molecule is disordered between two conformations in the same ratio. The water molecule bridges two independent M molecules via O-H...O, N-H...O and O-H...N hydrogen bonds into a 2M·H₂O unit, and these units are further linked by N-H...N hydrogen bonds into chains running in the [010] direction. Weak C-H...O interactions are observed between the adjacent chains. | fi |
| dc.language.iso | eng | |
| dc.publisher | International Union of Crystallography | |
| dc.relation.ispartofseries | Acta Crystallographica Section E : Structure Reports Online | |
| dc.relation.uri | http://dx.doi.org/10.1107/S160053681302713X | |
| dc.subject.other | N-[2-(2 | |
| dc.subject.other | 2-Dimetyylipropaaniamido)-pyrimidin-4-yyli]-2 | |
| dc.subject.other | 2-dimetyyli-propaaniamidi | |
| dc.subject.other | heksaanisolvaatti | |
| dc.subject.other | hemihydraatti | |
| dc.subject.other | kiderakenne | |
| dc.subject.other | 2-Dimethylpropanamido)-pyrimidin-4-yl]-2 | |
| dc.subject.other | 2-dimethyl-propanamide | |
| dc.subject.other | hexane solvate | |
| dc.subject.other | hemihydrate | |
| dc.subject.other | crystal structure | |
| dc.title | N-[2-(2,2-Dimethylpropanamido)- pyrimidin-4-yl]-2,2-dimethyl- propanamide n-hexane 0.25-solvate hemihydrate | |
| dc.type | article | |
| dc.identifier.urn | URN:NBN:fi:jyu-201310132463 | |
| dc.contributor.laitos | Kemian laitos | fi |
| dc.contributor.laitos | Department of Chemistry | en |
| dc.contributor.oppiaine | Orgaaninen kemia | fi |
| dc.contributor.oppiaine | Organic Chemistry | en |
| dc.type.uri | http://purl.org/eprint/type/JournalArticle | |
| dc.date.updated | 2013-10-13T03:30:05Z | |
| dc.type.coar | journal article | |
| dc.description.reviewstatus | peerReviewed | |
| dc.format.pagerange | o1617-o1618 | |
| dc.relation.issn | 1600-5368 | |
| dc.relation.numberinseries | 11 | |
| dc.relation.volume | 69 | |
| dc.type.version | publishedVersion | |
| dc.rights.copyright | © the Authors. This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence. | |
| dc.rights.accesslevel | openAccess | fi |
| dc.rights.url | http://creativecommons.org/licenses/by/2.0/uk/legalcode | |
| dc.relation.doi | 10.1107/S160053681302713X |
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