Näytä suppeat kuvailutiedot

dc.contributor.authorKoivukorpi, Juha
dc.contributor.authorKolehmainen, Erkki
dc.date.accessioned2012-11-02T08:58:37Z
dc.date.available2012-11-02T08:58:37Z
dc.date.issued2011
dc.identifier.citationKoivukorpi, J., & Kolehmainen, E. (2011). Synthesis of Both Ionic Species of Ammonium Dithiocarbamate Derived Cholic Acid Moieties. Molecules, 16 (8), 6306-6312. doi:10.3390/molecules16086306 Retrieved from http://www.mdpi.com/journal/molecules/
dc.identifier.urihttps://jyx.jyu.fi/handle/123456789/40156
dc.description.abstractThe reaction of 3-aminopropylamide of cholic acid with CS₂ produced a bile acid derivative of dithiocarbamic acid which further formed an ammonium salt with another molecule of 3-aminopropylamide of cholic acid. The cationic 3-ammonium propylamide of cholic acid did not react further with CS₂ and the formed salt was stable in the reaction mixture, even when excess CS₂ was used. When the reaction was carried out in the presence of aqueous sodium hydroxide, only the bile acid derivative of sodium dithiocarbamate was formed. The dithiocarbamate derivatives were characterized by ¹H- and ¹³C-NMR spectroscopy and ESI-TOF mass spectrometry.fi
dc.language.isoeng
dc.publisherMDPI
dc.relation.ispartofseriesMolecules
dc.relation.urihttp://www.mdpi.com/journal/molecules
dc.subject.othercholic aciden
dc.subject.otherdithiocarbamateen
dc.subject.otherdithiocarbamateen
dc.subject.othersteroiden
dc.subject.otherNMR spectroscopyen
dc.subject.otheramineen
dc.titleSynthesis of Both Ionic Species of Ammonium Dithiocarbamate Derived Cholic Acid Moieties
dc.typeArticle
dc.identifier.urnURN:NBN:fi:jyu-201211022843
dc.contributor.laitosKemian laitosfi
dc.contributor.laitosDepartment of Chemistryen
dc.type.urihttp://purl.org/eprint/type/JournalArticle
dc.identifier.doi10.3390/molecules16086306
dc.type.coarjournal article
dc.description.reviewstatuspeerReviewed
dc.relation.issn1420-3049
dc.type.versionpublishedVersion
dc.rights.copyright© 2011 by the authors; licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution license.
dc.rights.accesslevelopenAccessfi
dc.rights.urlhttp://creativecommons.org/licenses/by/3.0/


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Näytä suppeat kuvailutiedot

© 2011 by the authors; licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution license.
Ellei muuten mainita, aineiston lisenssi on © 2011 by the authors; licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution license.