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dc.contributor.authorNauha, Elisa
dc.contributor.authorSaxell, Heidi
dc.contributor.authorNissinen, Maija
dc.contributor.authorKolehmainen, Erkki
dc.contributor.authorSchäfer, Ansgar
dc.contributor.authorSchlecker, Rainer
dc.date.accessioned2011-11-08T07:10:56Z
dc.date.available2011-11-08T07:10:56Z
dc.date.issued2009
dc.identifier.citationNauha, E., Saxell, H., Nissinen, M., Kolehmainen, E., Schäfer, A., & Schlecker, R. (2009). Polymorphism and versatile solvate formation of thiophanate-methyl. <em>CrystEngComm</em>, 11, 2536-2547. <a href="http://dx.doi.org/10.1039/B905511H">doi:10.1039/B905511H</a>
dc.identifier.otherTUTKAID_36678
dc.identifier.urihttps://jyx.jyu.fi/handle/123456789/36906
dc.description.abstractThe polymorphism of a fungicide, thiophanate-methyl (TM), was investigated with conventional solvent screening methods. Two polymorphs, the thermodynamically most stable form I and the less stable form II, were found. TM was also found to crystallize as a plethora of different solvates which produced mostly form II upon desolvation. The structures of form I and form II and the fourteen discovered solvates were solved by single crystal X-ray diffraction. The most stable forms were further characterized by powder diffraction, thermoanalytical (TG/DTA, DSC and thermomicroscopy) and spectroscopic (IR, Raman, ¹³C CP/MAS NMR) methods.
dc.language.isoeng
dc.relation.ispartofseriesCrystEngComm
dc.relation.urihttp://www.rsc.org/Publishing/Journals/CE/article.asp?doi=b905511h
dc.subject.otherpolymorphismen
dc.subject.othersolvateen
dc.subject.othercrystal formen
dc.subject.otherpolymorfiafi
dc.subject.othersolvaattifi
dc.subject.otherkidemuotofi
dc.titlePolymorphism and versatile solvate formation of thiophanate-methyl
dc.typeArticle
dc.identifier.urnURN:NBN:fi:jyu-2011110811638
dc.contributor.laitosKemian laitos
dc.contributor.oppiaineOrgaaninen kemiafi
dc.contributor.oppiaineDepartment of Chemistryen
dc.type.urihttp://purl.org/eprint/type/SubmittedJournalArticle
dc.identifier.doi10.1039/B905511H
dc.date.updated2011-11-08T04:30:13Z
dc.contributor.publisherRoyal Society of Chemistry
dc.type.coarjournal article
dc.description.reviewstatuspeerReviewed
dc.format.pagerange2536-2547
dc.relation.volume11
dc.type.versionacceptedVersion
dc.rights.copyright© The Royal Society of Chemistry. This is an electronic final draft version of the article whose final and definitive form has been published in CrystEngcomm.
dc.rights.accesslevelopenAccessfi


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